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| U | Espanyol | - | FC Barcelona | 1:2 (0:2) | ||
| R | FC Barcelona | - | Espanyol | 1:1 (1:1) | ||
| U: 30.01.2001 21:30 | R: 07.02.2001 21:00 | Winnaars: FC Barcelona | ||||
| U | Racing Santander | - | Real Zaragoza | 1:1 (0:1) | ||
| R | Real Zaragoza | - | Racing Santander | 2:0 (1:0) | ||
| U: 31.01.2001 20:45 | R: 07.02.2001 21:00 | Winnaars: Real Zaragoza | ||||
| U | Celta de Vigo | - | RCD Mallorca | 3:1 (0:1) | ||
| R | RCD Mallorca | - | Celta de Vigo | 2:1 (1:0) | ||
| U: 31.01.2001 21:15 | R: 07.02.2001 21:00 | Winnaars: Celta de Vigo | ||||
| U | Granada CF | - | Atlético Madrid | 0:1 (0:1) | ||
| R | Atlético Madrid | - | Granada CF | 3:1 (1:0) | ||
| U: 31.01.2001 21:15 | R: 06.02.2001 21:30 | Winnaars: Atlético Madrid | ||||
